数字农科院2.0

Simultaneous Determination of 6 Neonicotinoid Residues in Soil Using DLLME-HPLC and UV

文献类型： 外文期刊

作者： Sun Bao-li;Shan Hong;Li Yan-hua;Zeng Ya-ling;Shen Xiu-li;Tong Cheng-feng

作者机构：

关键词： HPLC;UV;Dispersive liquid-liquid micro-extraction;Neonicotinoid;Soil

期刊名称： SPECTROSCOPY AND SPECTRAL ANALYSIS

ISSN： 1000-0593

年卷期： 2013 年 33 卷 9 期

页码：

收录情况： SCI

摘要： A simple, cheap and rugged method was developed for simultaneous deter mination of 6 neonicotinoid residues in soil, including imidacloprid, acetamiprid, thiamethoxam, thiacloprid, clothianidin and nitenpyram. The soil sample was produced by dispersive liquid-liquid micro-extraction (DLLME) after extracted by the mixed solution of acetonitrile and CH2Cl2 (2 1, phi). The analytes were separated by HPLC with Alltima (TM) C-18 column (4. 6 mmX 250 mm, 5 mu m) and detected by PDA at 260 tun. External standard method was used for quantification. The results showed that good linearity was obtained with correlation coefficients between 0. 998 2 and 0. 999 9 in the range of 0. 5 similar to 200 mu g.L-1. The limits of detection (LODs) were in the range between 0. 000 5 and 0. 003 mu g.mL(-1) (S/N=3). The method was validated with five soil samples spiked at three fortification levels (0. 05, 0. 1, 1.0 mg.kg(-1)) and recoveries were in the range of 55. 3%similar to 95. 6% with RSD of 1. 4%similar to 7. 0%. The effect of clean-up was evaluated by UV spectra and demonstrated that the method established is effective. In conclusion, this method is competent for the simultaneous analysis of 6 neonicotinoid residues in soil.

分类号：

  • 相关文献

[1]High Performance Liquid Chromatography determination of Fentin Acetate Residue in Beet and Soil. Sun Hui-qing,Li Yi-qiang,Xu Guang-jun,Zheng Xiao,Xu Jin-li,Wang Xiu-guo. 2012

[2]Enantioselective Degradation of Chiral Insecticide Dinotefuran in Greenhouse Cucumber and Soil. Dong, Fengshou,Xu, Jun,Liu, Xingang,Wang, Yunhao,Zheng, Yongquan,Chen, Xiu.

[3]Preliminary Study of the Characterization of the Viable but Noncultivable State of Yersinia enterocolitica Induced by Chloride and UV Irradiation. Xueyu Hu,Xiaoxu Wang,Honglin Ren,Chengwei Li,Bo Zhang,Ruoran Shi,Yuzhu Wang,Shiying Lu,Yansong Li,Qiang Lu,Zengshan Liu,Pan Hu. 2024

[4]A PHR-dependent reciprocal antagonistic interplay between UV response and P-deficiency adaptation in plants. Ren, Jianhao,Li, Tianjie,Guo, Meina,Zhang, Qianqian,Ren, Suna,Wang, Long,Wu, Qingyu,Niu, Shihui,Yi, Keke,Ruan, Wenyuan. 2025

[5]Design, synthesis and insecticidal activity of novel hydrocarbylidene nitrohydrazinecarboximidamides. Yang, Dong-yan,Zhou, Zi-yuan,Ma, Yong-qiang,Qin, Zhao-hai,Zou, Xiang-gao,Rui, Chang-hui.

[6]Systemic action of novel neonicotinoid insecticide IPP-10 and its effect on the feeding behaviour of Rhopalosiphum padi on wheat. Cui, Li,Sun, Lina,Cao, Yazhong,Yang, Daibin,Yuan, Huizhu,Shao, Xusheng,Li, Zhong.

[7]Determination of neonicotinoid insecticides residues in eels using subcritical water extraction and ultra-performance liquid chromatography-tandem mass spectrometry. Xiao, Zhiming,Yang, Yunxia,Li, Yang,Fan, Xia,Ding, Shuangying.

[8]Toxicity of Insecticides Targeting Rice Planthoppers to Adult and Immature Stages of Trichogramma chilonis (Hymenoptera: Trichogrammatidae). Liu, Yudi,Hou, Maolin,Babendreier, Dirk,Zhang, Feng,Song, Kai.

[9]Lethal effect of imidacloprid on the coccinellid predator Serangium japonicum and sublethal effects on predator voracity and on functional response to the whitefly Bemisia tabaci. Wu, Kongming,He, Yuxian,Zhao, Jianwei,Zheng, Yu,Desneux, Nicolas. 2012

[10]Urinary Monitoring Of Neonicotinoid Imidacloprid E.xposure To Pesticide Applicators. Wu, Xiaohu,Liu, Qianyu,Liu, Xingang,Tao, Yan,Pan, Xinglu,Zheng, Yongquan,Li, Runan,He, Min,Dong, Fengshou,Xu, Jun,Dung Phung. 2019

[11]Assessing the effectiveness of imidacloprid and thiamethoxam via root irrigation against Megalurothrips usitatus (Thysanoptera: Thripidae) and its residual effects on cowpea. Yu, Xiao-Rui,Tariq, Talha,Guo, Ling-Hang,Wu, Sheng-Yong,Tang, Liang-De,Zang, Lian-Sheng. 2023

[12]Facile Three-Component Synthesis, Insecticidal And A.ntifungal Evaluation Of Novel D ihydropyridine Derivatives. Yang, GZ, Shang, XF, Cheng, PL, Yin, XD, Zhu, JK, Liu, YQ, Zhang, J, Zhang, ZJ. 2018

[13]Transgenerational effects of a neonicotinoid and a novel sulfoximine insecticide on the harlequin ladybird. Changchun Dai,Michele Ricupero,Zequn Wang,Nicolas Desneux,Antonio Biondi,Yanhui Lu. 2021

[14]ZIF-8 and humic acid modified magnetic corn stalk biochar: An efficient, magnetically stable, and eco-friendly adsorbent for imidacloprid and thiamethoxam removal. Yong Yang,Xinxin Ma,Zifen Li,Yanru Wang,Chao Ju,Lidong Cao,Yongquan Zheng,Qingming Zhang. 2023

[15]CYP6CX2 and CYP6CX3 mediate thiamethoxam resistance in field whitefly, Bemisia tabaci (Hemiptera:Aleyrodidae). Yang, Jing,Fu, Buli,Gong, Peipan,Zhang, Chengjia,Wei, Xuegao,Yin, Cheng,Huang, Mingjiao,He, Chao,Du, Tianhua,Liang, Jinjin,Liu, Shaonan,Ji, Yao,Xue, Hu,Wang, Chao,Hu, Jinyu,Du, He,Zhang, Rong,Yang, Xin,Zhang, Youjun. 2023

[16]The water-exiting behavior and survival of predaceous diving beetles in responses to lambda-cyhalothrin, chlorantraniliprole, and thiamethoxam. Wang L.,Liu L.,Feng S.. 2024

[17]Precise Control and Prevention Methods for Whitefly in Greenhouse Vegetables. Xiaoyan Dai,Qingcai Lin,Yan Liu,Ruijuan Wang,Long Su,Zhenjuan Yin,Shan Zhao,Feng Zhang,Hao Chen,Li Zheng,Yifan Zhai,Lisheng Zhang. 2024

[18]CRISPR/Cas9-mediated mutation of nicotinic acetylcholine receptor (nAChR) α subunit confers moderate levels of resistance to spinosad and imidacloprid in the natural predator Coccinella septempunctata without fitness cost. Guo, Xingkai,Zhang, Lisheng,Wang, Mengqing,Li, Yuyan,Shen, Zhongjian,Nolan, Tony,Mao, Jianjun. 2024

[19]Sublethal effects of thiamethoxam on Encarsia formosa: intergenerational impacts and insights from transcriptomic analysis. Wang, Ke,He, Yanyan,Zhang, Yan,Dong, Rui,Hu, Shouyin,Yang, Zezhong,Guo, Zhaojiang,Zhang, Youjun,Xie, Wen,Wang, Shaoli. 2025

[20]Molecular mechanisms of cis-oxygen bridge neonicotinoids to Apis mellifera Linnaeus chemosensory protein: Surface plasmon resonance, multiple spectroscopy techniques, and molecular modeling. Xiangshuai Li,Shiyu Li,Yang Liu,Li Cui,Daibin Yang,Shuning Chen,Xusheng Shao,Huizhu Yuan,Xiaojing Yan. 2025

作者其他论文 更多>>