数字农科院2.0

Determination of Polycyclic Aromatic Hydrocarbons and Halogenated Polycyclic Aromatic Hydrocarbons in Vegetable by Gas Chromatography-Tandem Mass Spectrometry

文献类型： 外文期刊

作者： Wang Li;Jiao Bi-Ning;Wang Li;Jin Fen;Li Min-Jie;Shao Hua;Jin Mao-Jun;Wang Jing;Wang Li;Jiao Bi-Ning;Liu Yue

作者机构：

关键词： Polycyclic aromatic hydrocarbons;Halogenated polycyclic aromatic hydrocarbons;Gas chromatography tandem mass spectrometry;Dispersive solid phase extraction;Vegetables

期刊名称： CHINESE JOURNAL OF ANALYTICAL CHEMISTRY

ISSN： 0253-3820

年卷期： 2013 年 41 卷 6 期

页码：

收录情况： SCI

摘要： A method was developed for determination of 16 polycyclic aromatic hydrocarbons and 11 halogenated polycyclic aromatic hydrocarbons in vegetables by gas chromatography. tandem mass spectrometry(GC-MS/MS). The analytes were extracted from the vegetable samples by hexane, and purified by dispersion solid phase extraction using PSA and C-18 sorbent, then analyzed by gas chromatography. tandem mass spectrometry (GC-MS/MS) with external standard method. The recoveries were in the range of 74. 7% -115. 1%, and the relative standard deviations (RSD) were 1. 6% -15. 3% at three spiked levels of 50,100 and 200 mu g/kg for 16 polycyclic aromatic hydrocarbons and 11 halogenated polycyclic aromatic hydrocarbons. The limits of quantification (LOQ) for all analytes were 0. 03-7. 39 mu g/kg.

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