数字农科院2.0

A simple and economic method for simultaneous determination of 11 antibiotics in manure by solid-phase extraction and high-performance liquid chromatography

文献类型： 外文期刊

作者： Feng, Yao;Zhang, Wenjuan;Liu, Yuanwang;Li, Zhaojun;Hu, Haiyan;Wei, Chaojun;Zhang, Wenjuan;Xue, Jianming

作者机构：

关键词： Antibiotics;Determination;High-performance liquid chromatography;Manures;Solid-phase extraction

期刊名称： JOURNAL OF SOILS AND SEDIMENTS

ISSN： 1439-0108

年卷期： 2016 年 16 卷 9 期

页码：

收录情况： SCI

摘要： A simple and highly efficient economic method for the analysis of 11 antibacterial drugs including two tetracyclines, three quinolones, four sulfonamides, chloramphenicol and tylosin, in livestock manure, was developed using solid-phase extraction (SPE) and high-performance liquid chromatography (HPLC). The analytes were successively extracted by EDTA-McIlvaine solution and organic solvent mixture. The extracts were degreased with n-hexane and cleaned through SPE on a hydrophile-lipophile balance (HLB) cartridge. All compounds were determined on a C18 reverse phase column with gradient elution. Recoveries calculated from spiked samples of animal manures ranged from 62.65 to 99.16 % for 11 antibiotics with relative standard deviations of less than 10.0 %. Limits of detection ranged from 0.1 to 1.9 mu g kg(-1), and limits of quantification ranged from 0.3 to 5.9 mu g kg(-1). The results show that SPE-HPLC is an inexpensive and practical method for rapid detection of multiple antibiotics in animal manure.

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