CO2 -responsive deep eutectic solvents for the enhanced extraction of hesperidin from Fertile orange peel
文献类型： 外文期刊
作者： Wang, Shanshan;Lei, Tian;Liu, Leilei;Tan, Zhijian
作者机构：
关键词： CO 2-responsive deep eutectic solvents;Recyclable extractants;Extraction;Bioactive compounds;Hesperidin
期刊名称： FOOD CHEMISTRY
ISSN： 0308-8146
年卷期： 2024 年 432 卷
页码：
收录情况： SCIE（2024版） ; ; EI（2024版）
摘要： Hesperidin, also known as vitamin P, is widely studied for its distinctive potential in food and pharmaceutical industries. This work focuses on the research of CO2-responsive deep eutectic solvents (DESs) used as recyclable extractants for efficient extraction of hesperidin from Fertile orange peel. Reversible phase transformation of DES solution was achieved by bubbling CO2/N2. The maximum extraction yield of 22.39 mg/g was obtained for hesperidin under the following conditions: DES-6 (triethanolamine: 4-methoxyphenol = 1:1) used as extractant, water content of 35 wt%, solid-liquid ratio of 1:60 g/mL, extraction temperature of 25 degrees C, and ultrasonic time of 25 min, which was much higher than that extracted by methanol. Hesperidin of 74.38% was recovered in top phase after CO2 triggering. Density function theory (DFT) results indicated that hydrogen and & pi;-& pi; bonds were the main factors affecting hesperidin extraction. This study provides a new idea for extracting natural bioactive compounds using recyclable extractants.
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