数字农科院2.0

Rapid and simultaneous detection of lead and cadmium in foods using solid sampling electrothermal vaporization coupled with a composite MgO/ quartz trap

文献类型： 外文期刊

作者： Lan, Guanyu;Chen, Lin;Xu, Yan;Li, Xue;Feng, Li;Mao, Xuefei

作者机构：

关键词： Multi-elemental solid sampling;Lead;Cadmium;Foods;Composite MgO/quartz trap;Integrated electrothermal vaporization

期刊名称： TALANTA

ISSN： 0039-9140

年卷期： 2025 年 301 卷

页码：

收录情况： SCIE（2025版） ; ; EI（2025版）

摘要： This work constructed an innovative rapid multi-elemental analyzer of Pb and Cd using solid sampling electrothermal vaporization (ETV) with a composite trap based on the principle of gas phase enrichment (GPE). A SiO2-MgO-SiO2 sandwich-structured GPE unit was first fabricated to enable simultaneous capture and rapid thermal release of Pb and Cd. Mechanism studies demonstrated that temperature drives the distribution of Pb and Cd in GPE unit; lower temperature favors accumulation at the lower layer, while higher temperature promotes upper migration and may thus reduce trapping efficiency. Under optimized conditions, limits of detection (LODs) of 0.4-0.5 ng/g were achieved in 100 mg sample size. The linearity (R-2>0.999) and the recoveries (82-117 %) indicate excellent analytical precision and accuracy without requiring sample digestion. Rapid detection of Pb and Cd in various food matrices was accomplished with similar to 3 min. Thus, the proposed method is simple, green and robust, making it suitable for rapid monitoring of heavy metals in food.

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