数字农科院2.0

Determination of Aflatoxin B-1 and Aflatoxin B-2 in Edible Oil by Using Graphene Oxide-SiO2 as Soild Phase Extraction Coupled with HPLC

文献类型： 外文期刊

作者： Wang Heng-Ling;Yu Li;Li Pei-Wu;Li Min;Zhang Qi;Zhang Wen;Wang Heng-Ling;Yu Li;Li Pei-Wu;Li Min;Zhang Wen;Wang Heng-Ling;Li Pei-Wu;Li Min;Zhang Qi;Yu Li;Li Pei-Wu;Zhang Qi

作者机构：

关键词： Silica dioxide bound graphene oxide;Solid phase extraction;Aflatoxins;Edible oil;High performance liquid chromatography

期刊名称： CHINESE JOURNAL OF ANALYTICAL CHEMISTRY

ISSN： 0253-3820

年卷期： 2014 年 42 卷 9 期

页码：

收录情况： SCI

摘要： Silica dioxide bound graphene oxide (GO-SiO2) was applied as an effective adsorbent for determination and quantiflcation of aflatoxin B-1, B-2 in edible oil by HPLC. The optimized conditions were GO-SiO2 0.15 g, extraction time 20 min, elution reagent acetonitrile, elution cycles two times. Results showed under the optimum conditions, the detection limits of aflatoxin B-1, B-2 were 0.17 and 0.05 mu g/L, respectively. The method was successfully applied to the detection of the actual edible oil, the spiked recoveries of aflatoxin B-1 and B-2 were 81.4%-105.3% and the relative standard deviations were 1.3%-8.6%.

分类号：

  • 相关文献

[1]Effervescence-assisted dispersive liquid-liquid microextraction using a solid effervescent agent as a novel dispersion technique for the analysis of fungicides in apple juice. Jiang, Wenqing,Chen, Xiaochu,Liu, Fengmao,You, Xiangwei,Xue, Jiaying,You, Xiangwei.

[2]Analysis of coenzyme Q10 in bee pollen using online cleanup by accelerated solvent extraction and high performance liquid chromatography. Xue, Xiaofeng,Liu, Fengmao,Xue, Xiaofeng,Zhao, Jing,Chen, Lanzhen,Zhou, Jinhui,Yue, Bing,Li, Yi,Wu, Liming,Xue, Xiaofeng,Zhao, Jing,Chen, Lanzhen,Zhou, Jinhui,Yue, Bing,Li, Yi,Wu, Liming.

[3]Interbatch quality control of the extract from Artemisia frigida Willd. by spectrum-effect relationship between HPLC fingerprints and the total antioxidant capacity. Tian, Wei,Yang, Juan,Dou, Jiahong,Li, Xiumei,Dai, Xiaofeng,Wang, Xiumin,Sun, Yahong,Li, Zhongyuan. 2022

[4]Terpenoids identification and authenticity evaluation of longan, litchi and schefflera honey. Hequan Zhu,Yinan Du,Xun Lin,Zhonglian Huang,Jie Dong,Jiangtao Qiao,Hongcheng Zhang. 2025

[5]Simultaneous determination of triazine herbicides in rice by high-performance liquid chromatography coupled with high resolution and high mass accuracy hybrid linear ion trap-orbitrap mass spectrometry. Mou, Ren-Xiang,Chen, Ming-Xue,Cao, Zhao-Yun,Zhu, Zhi-Wei.

[6]Assessment of primary and secondary amine adsorbents and elution solvents with or without graphitized carbon for the SPE clean-up of food extracts in pesticide residue analysis. He, Yan,Liu, Yan-Hong. 2007

[7]Simultaneous Determination of 14 Kinds of beta-Agonist Residues in Sheep Saliva by Ultra Performance Liquid Chramatogrephy-Tandem Mass Spectrometry. Li Yang,Su Xiao-Ou,Wang Rui-Guo,Wang Pei-Long,Zhang Wei,Chen Jie. 2013

[8]Determination of Tetracyclines and Their Epimers in Agricultural Soil Fertilized with Swine Manure by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry. Zheng Wen-li,Zhang Li-fang,Zhang Ke-yu,Wang Xiao-yang,Xue Fei-qun. 2012

[9]Simultaneous determination of 10 first-generation histamine h1 receptor blockers in feeds by ultra-high-performance liquid chromatography triple quadrupole ion trap hybrid mass spectrometer. Suo, Decheng,Xia, Fan,Xiao, Zhiming,Yang, Li,Shi, Wang. 2023

[10]Rapid Purification and Quantification of Intestinal and Fecal Short-Chain Fatty Acids by Solid-Phase Extraction Using Bond Elut Plexa. Xing Zheng,Tao Chen,Wanli Li,Kai Wang,Xiaofeng Xue,Nenad Naumovski,Wenjun Peng. 2024

[11]An improved method for the measurement of 3-monochloropropanediol esters by matrix solid-phase dispersionsupported liquid-liquid extraction. Jiao, Bo,Hu, Hui,Shi, Aimin,Liu, Hongzhi,Liu, Li,Wang, Qiang,Fu, Wusheng,Adhikari, Benu.

[12]Simultaneous Determination of Perfluorinated Compounds in Edible Oil by Gel-Permeation Chromatography Combined with Dispersive Solid-Phase Extraction and Liquid Chromatography-Tandem Mass Spectrometry. Yang, Lili,Jin, Fen,Zhang, Peng,Zhang, Yanxin,Wang, Jian,Shao, Hua,Jin, Maojun,Wang, Shanshan,Zheng, Lufei,Wang, Jing.

[13]Rapid Magnetic Solid-Phase Extraction Based on Magnetic Multiwalled Carbon Nanotubes for the Determination of Polycyclic Aromatic Hydrocarbons in Edible Oils. Zhao, Qin,Luo, Yan-Bo,Ding, Jun,Xiao, Neng,Feng, Yu-Qi,Wei, Fang.

[14]Classification and Adulteration Detection of Vegetable Oils Based on Fatty Acid Profiles. Zhang, Liangxiao,Li, Peiwu,Sun, Xiaoman,Wang, Xuefang,Xu, Baocheng,Wang, Xiupin,Ma, Fei,Zhang, Qi,Ding, Xiaoxia,Ma, Fei,Zhang, Qi,Li, Peiwu,Zhang, Qi,Zhang, Liangxiao,Li, Peiwu,Ding, Xiaoxia,Zhang, Liangxiao,Li, Peiwu,Sun, Xiaoman,Wang, Xuefang,Xu, Baocheng,Wang, Xiupin,Ma, Fei.

[15]Diacylglycerols ions as novel marker indicators for the classification of edible oils using ultrahigh resolution mass spectrometry. Yanfen Zhang,Yehua Han,Wenya Hu,Qiong Pan,Zhanfang Liu,Guannan Ling,Quan Shi,Rui Weng. 2021

[16]A sensitive intelligent point-of-care test method for tert-butylhydroquinone in edible oil via a test strip with a smartphone. Dan Wang,Le Zhang,Jing Zeng,Shenling Wang,Wangwang Li,Yuanlong Sun,Wenqin Wu,Zhi Quan Tian,Zhaowei Zhang. 2024

[17]Adulteration detection of edible oil by one-class classification and outlier detection. Dou, Xinjing,Tu, Fengqin,Yu, Li,Yang, Yong,Ma, Fei,Wang, Xuefang,Wang, Du,Zhang, Liangxiao,Jiang, Xiaoming,Li, Peiwu. 2024

[18]A stable and reusable aluminum-based metal-organic framework for the effective extraction of four aflatoxins from vegetable oils. Xianhong Jiang,Jie Cheng,Zhihui Yang,Peilong Wang. 2025

[19]Visible light-driven activation of peroxymonosulfate by tubular O, S co-doped g-C3N4 for efficient aflatoxin B1 degradation in edible oils. Chen Hu,Chao Yang,Yihu Wang,Bo Li,Bangzhu Peng. 2025

[20]Authentication of Edible Oil by Real-Time One Class Classification Modeling. Min Liu,Xueyan Wang,Yong Yang,Fengqin Tu,Li Yu,Fei Ma,Xuefang Wang,Xiaoming Jiang,Xinjing Dou,Peiwu Li,Liangxiao Zhang. 2025

作者其他论文 更多>>