数字农科院2.0

Simultaneous Determination of Sodium Pentachlorophenolate and Its Metabolites in Swine Samples

文献类型： 外文期刊

作者： Qi Jia;Miao Cui;Meiling Li;Yuncheng Li;Fanbing Meng;Yanyang Xu;Yongzhong Qian;Xue Yan;Jing Qiu

作者机构：

关键词： chromatography tandem mass spectrometry;metabolites;residue detection;sodium pentachlorophenolate;swine samples

期刊名称： Separations

ISSN： 2297-8739

年卷期： 2023 年 10 卷 10 期

页码：

收录情况： SCIE（2023版）

摘要： Pentachlorophenol (PCP) is a persistent organic pollutant usually present in the form of sodium salts (PCP-Na) that has been banned for many years, but it can still be detected in animal food. The present study established a method of detecting PCP-Na and its metabolites—tetrachlorocatechol (TCC), pentachlorophenol acetate (PCP-acetate), and pentachloroanisole (PCA)—in swine samples (pork, fat, liver, heart, lungs and kidney), simultaneously using liquid chromatography-tandem mass spectrometry (LC-MS/MS) and gas chromatography-tandem mass spectrometry (GC-MS/MS) based on the modified QuEChERS pre-treatment method. The validation results exhibited a good sensitivity with limits of quantitation (LOQs) of 1 μg/kg–2 μg/kg. The recoveries of spiked samples were in the range of 60.5–119.9%, with a relative standard deviation (RSD) between replicates (n = 5) of between 0.70% and 12.06%.

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