数字农科院2.0

Determination of 9 Biological Amines and 2 Organic Amines in Fish Meat by Precolumn Derivatization Liquid Chromatography-Tandem Mass Spectrometry Based on Hinsberg Reaction

文献类型： 外文期刊

作者： He, Xiwen;Lei, Hao;Zhao, Juan;Wang, Junming;Li, Songli;Li, Hong;Zhao, Caihui

作者机构：

关键词： Biological amines;Organic amines;Fish meat;Precolumn derivatization;Liquid chromatography-tandem mass spectrometry;Hinsberg reaction

期刊名称： FOOD ANALYTICAL METHODS

ISSN： 1936-9751

年卷期： 2023 年

页码：

收录情况： SCIE（2023版） ; ; EI（2023版）

摘要： Multiple studies have demonstrated the harmful effects of consuming high levels of biogenic amines (BAs) and organic amines (OAs), underscoring the need for precise monitoring techniques. This study presents an innovative precolumn derivatization high-performance liquid chromatography-tandem mass spectrometry approach, utilizing the Hinsberg reaction, which can accurately detect 9 BAs and 2 OAs in fish meat with excellent sensitivity. BAs and OAs in fish meat were extracted using 5% trichloroacetic acid solution. Add dansyl chloride-acetonitrile solution (5 mg mL(-1)) and react in the dark at 45 & DEG;C water bath temperature for 30 min. The derivative products were analyzed on a liquid chromatography-tandem mass spectrometer. The results presented in this study provide excellent RSDs of 0.7-5.4% and great linear relationship (R-2 > 0.99) for 9 BAs and 2 OAs; high recoveries were obtained in different fish samples (79.4-101.4%). This study provides new analytical methods for BAs and OAs, providing a solution to the potential hazards of these amines in fish meat.

分类号：

  • 相关文献

[1]Determination of 26 Mycotoxins in Feedstuffs by Multifunctional Clean-up Column and Liquid Chromatography-Tandem Mass Spectrometry. Wang Rui-Guo,Su Xiao-Ou,Cheng Fang-Fang,Wang Pei-Long,Fan Xia,Zhang Wei. 2015

[2]Determination of Trace Atrazine and Two Kinds of Its Metabolites in Milk by Solid Phase Extraction and Liquid Chromatography/Mass Spectrometry. Shi Dong-Dong,Liu Qing-Sheng,Shi Bo,Chang Bi-Ying. 2013

[3]Liquid Chromatography-Tandem Mass Spectrometry for Determination of Aflatoxin B-1, Deoxynivalenol and Zearalenone in Artificial Porcine Gastrointestinal Digestive Juice. Wang Rui-Guo,Su Xiao-Ou,Fan Xia,Wang Pei-Long,Gao Zhong-Wu,Zhang Yu. 2015

[4]Simultaneous Determination of Seven Mental Drugs in Feeds by Liquid Chromatography-Tandem Mass Spectrometry. Suo De-Cheng,Zhao Gen-Long,Li Lan,Su Xiao-Ou. 2010

[5]Determination of 19 Acidic Pesticide Residues in Fruit by Dispersive Solid Phase Extraction and Liquid Chromatography-Tandem Mass Spectrometry. Jin Fen,Shi Xiao-Mei,Li Min-Jie,Shao Hua,Jin Mao-Jun,Wang Jing,Yu Zhi-Yong. 2013

[6]Simultaneous Determination of 11 Phenolic Compounds in Perilla oil by High Performance Liquid Chromatography-Tandem Mass Spectrometry. Wu Rao,Ma Fei,Zhang Liang-Xiao,Li Pei-Wu,Zhang Wen,Zhang Qi,Li Guang-Ming,Wu Rao,Li Guang-Ming,Li Pei-Wu,Zhang Qi,Zhang Liang-Xiao,Li Pei-Wu,Ma Fei,Zhang Liang-Xiao,Li Pei-Wu,Zhang Wen,Li Guang-Ming. 2015

[7]Proteomics Analysis of Porcine Serum Proteins by LC-MS/MS after Foot-and-Mouth Disease Virus (FMDV) Infection. Liu, Yongjie,Zhang, Keshan,Zheng, Haixue,Shang, Youjun,Guo, Jianhong,Tian, Hong,Lu, Guodong,Jin, Ye,He, Jijun,Cai, Xuepeng,Li, Xiangtao.

[8]Rapid determination of trans-resveratrol in vegetable oils using magnetic hydrophilic multi-walled carbon nanotubes as adsorbents followed by liquid chromatography-tandem mass spectrometry. Ma, Fei,Li, Peiwu,Zhang, Qi,Yu, Li,Zhang, Liangxiao,Ma, Fei,Li, Peiwu,Zhang, Qi,Yu, Li,Zhang, Liangxiao,Ma, Fei,Li, Peiwu,Zhang, Qi,Yu, Li,Zhang, Liangxiao,Ma, Fei,Li, Peiwu,Yu, Li,Zhang, Liangxiao,Li, Peiwu,Zhang, Qi.

[9]Simultaneous determination of 13 phytohormones in oilseed rape tissues by liquid chromatography-electrospray tandem mass spectrometry and the evaluation of the matrix effect. Fan, Sufang,Wang, Xiupin,Li, Peiwu,Zhang, Qi,Zhang, Wen,Fan, Sufang,Wang, Xiupin,Li, Peiwu,Zhang, Qi,Zhang, Wen,Fan, Sufang,Wang, Xiupin,Li, Peiwu.

[10]Simultaneous determination of phenolic compounds in sesame oil using LC-MS/MS combined with magnetic carboxylated multi-walled carbon nanotubes. Wu, Rao,Ma, Fei,Zhang, Liangxiao,Li, Peiwu,Li, Guangming,Zhang, Qi,Zhang, Wen,Wang, Xiuping,Wu, Rao,Ma, Fei,Zhang, Liangxiao,Li, Peiwu,Li, Guangming,Zhang, Qi,Wang, Xiuping,Wu, Rao,Ma, Fei,Li, Peiwu,Li, Guangming,Zhang, Qi,Wang, Xiuping,Wu, Rao,Ma, Fei,Zhang, Liangxiao,Li, Peiwu,Zhang, Wen,Wang, Xiuping,Zhang, Liangxiao,Li, Peiwu,Li, Guangming,Zhang, Qi,Zhang, Wen,Zhang, Liangxiao,Zhang, Wen.

[11]Simultaneous Detection Of 21 Kinds O.f Mycotoxins And Their M etabolites In Animal Plasma With Impurity Adsorption Purification Followed By Liquid Chromatography-Tandem Mass Spectrometry. Wang, RG, Su, XO, Wang, PL, Zhang, W, Xue, Y, Li, Y. 2017

[12]Determination of acetylgestagens in animal-derived matrix samples using enhanced matrix removal lipid clean-up in combination with ultra performance liquid chromatography-tandem mass spectrometry. Congcong Zhang,Qingyang Zhang,Zenghao Yin,Jian Hu,Gang Chen,Lufei Zheng,Aijin Ma. 2021

[13]Development and Validation for Simultaneous Determination of Disulfoton and Its Five Metabolites in Seven Agro-Products Using Liquid Chromatography-Tandem Mass Spectrometry Combined with QuEChERS Extraction Method. Li, Hui,Pan, Lingyi,Yu, Chunsheng,Zhang, Xukun,Cui, Xueyan,Luo, Ting,Cao, Zhen,Wang, Jing,Li, Qingxiao. 2022

[14]Integrating a Multiple Isotopologue Reaction-Monitoring Technique and LC-MS/MS for Quantitation of Small Molecules: Ten Mycotoxins in Cereals as an Example. Feifei Sun,Yanshen Li,Haiguang Tan,Peixu Wu,Yingnan Shencheng,Haopeng Lin,Peng Lu,Rong Zhang,Shuyan Liu,Yi Li,Shupeng Yang. 2024

[15]Simultaneous determination of 58 glucocorticoid residues in milk by ultra-high performance liquid chromatography-tandem mass spectrometry. Guo C.,Wu C.,Zhang Z.,Tan S.,Chen S.,Chen G.. 2024

[16]A stable and reusable aluminum-based metal-organic framework for the effective extraction of four aflatoxins from vegetable oils. Xianhong Jiang,Jie Cheng,Zhihui Yang,Peilong Wang. 2025

作者其他论文 更多>>